2-{9-(10-Bromoanthracenyl)}-1,3-dihydro-1H-[d]-1,3,2-benzodiazaborole

نویسندگان

چکیده

In this paper, a synthesis and characterization of novel three coordinate 2-{9-(10-Bromoanthracenyl)}-1,3-dihydro-1H-[d]-1,3,2-benzodiazaborole from cyclo-condensation reaction o-phenylenediamine 10-bromoanthracene-9-boronic acid is described. The desired product was obtained in 0.343 g (92% yields) with its structure characterized by 1H, 11B, 13C NMR, HRMS FT-IR.

برای دانلود باید عضویت طلایی داشته باشید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

2-(2-Thien­yl)-4,5-dihydro-1H-imidazole

In title compound, C(7)H(8)N(2)S, the five-membered rings are twisted by a dihedral angle of 5.17 (10)°. Two inter-molecular N-H⋯N and C-H⋯N hydrogen bonds to the same acceptor N atom form seven-membered rings, producing R(2) (1)(7) ring motifs. These inter-actions link neighbouring mol-ecules into one-dimensional chains extended along the c axis. The crystal structure is further stabilized by ...

متن کامل

2-[4-(4,5-Dihydro-1H-pyrrol-2-yl)phen­yl]-4,5-dihydro-1H-imidazole

The mol-ecule of the title compound, C(12)H(14)N(4), lies about a crystallographic inversion centre. The five- and six-membered rings are twisted from each other, forming a dihedral angle of 18.06 (7)°. In the crystal structure, neighbouring mol-ecules are linked by inter-molecular N-H⋯N hydrogen bonds into one-dimensional infinite chains forming 18-membered rings with R(2) (2)(18) motifs. The ...

متن کامل

2-[4-(4,5-Dihydro-1H-pyrrol-2-yl)phen­yl]-4,5-dihydro-1H-imidazole. Corrigendum

The chemical name of the title compound in the paper by Kia, Fun & Kargar [Acta Cryst. (2009), E64, o2406] is corrected.[This corrects the article DOI: 10.1107/S1600536809023320.].

متن کامل

2-(3-Chloro­phen­yl)-4,5-dihydro-1H-imidazole

In the title compound, C(9)H(9)ClN(2), a substituted imidazoline, the six- and five-membered rings are twisted from each other, making a dihedral angle of 17.07 (5)°. In the crystal structure, a short Cl⋯Cl [3.3540 (3) Å] inter-action is observed. Neighbouring mol-ecules are linked together by inter-molecular N-H⋯N hydrogen bonds into a one-dimensional infinite chain along the [101] direction a...

متن کامل

2-(4-Methoxy­phen­yl)-4,5-dihydro-1H-imidazole

In the title mol-ecule, C(10)H(12)N(2)O, the dihedral angle between the benzene and imidazole rings is 14.86 (16)°. The approximately planar arrangement of the mol-ecule results in a distance of 2.54 Å between an ortho-H atom of the benzene ring and the double-bonded N atom of the imidazole ring. In the crystal structure, symmetry-related mol-ecules are linked by inter-molecular N-H⋯N hydrogen ...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

ژورنال

عنوان ژورنال: Molbank

سال: 2023

ISSN: ['1422-8599']

DOI: https://doi.org/10.3390/m1569